Isolation and identification of phenolic compounds in Citrus sinensis
Identifieur interne : 002F28 ( Main/Exploration ); précédent : 002F27; suivant : 002F29Isolation and identification of phenolic compounds in Citrus sinensis
Auteurs : Prasan Swatsitang [Royaume-Uni] ; Greg Tucker [Royaume-Uni] ; Kevin Robards [Australie] ; Daniel Jardine [Australie]Source :
- Analytica Chimica Acta [ 0003-2670 ] ; 2000.
Descripteurs français
- Pascal (Inist)
- Analyse chimique, Analyse multiélément, Analyse quantitative, Chromatographie phase inverse, Chromatographie phase liquide, Citrus sinensis, Contrôle qualité, Electrospray, Hydrolyse, Industrie boisson, Ionisation chimique, Jus d'orange, Méthode couplée, Phénol dérivé, Phénols, Pression atmosphérique, Préparation échantillon, Solution basique, Spectrométrie masse, Traitement chimique.
- Wicri :
- topic : Analyse quantitative.
English descriptors
- KwdEn :
- Atmospheric pressure, Basic solution, Beverage industry, Chemical analysis, Chemical ionization, Chemical treatment, Citrus, Citrus sinensis, Coupled method, Electrospray, HPLC, Hydrolysis, Liquid chromatography, Mass spectrometry, Multicomponent analysis, Orange juice, Phenols, Quality control, Quantitative analysis, Reversed phase chromatography, Sample preparation.
Abstract
Various methods were compared for the recovery of phenolic compounds from sweet orange. The need for careful consideration of sample preparation was demonstrated. In the case of cinnamic acids, hydroxide-treatment was essential to liberate the bound acids. Ferulic acid was the predominant phenol in alkali-treated extracts. Positive and negative ion electrospray ionisation mass spectra were systematically investigated for a range of phenols. Detection limits were significantly lower in negative ion than in positive ion mode. However, positive ion mode provided additional structural information for many of the compounds.
Url:
DOI: 10.1016/S0003-2670(00)00937-5
Affiliations:
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Le document en format XML
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<front><div type="abstract" xml:lang="en">Various methods were compared for the recovery of phenolic compounds from sweet orange. The need for careful consideration of sample preparation was demonstrated. In the case of cinnamic acids, hydroxide-treatment was essential to liberate the bound acids. Ferulic acid was the predominant phenol in alkali-treated extracts. Positive and negative ion electrospray ionisation mass spectra were systematically investigated for a range of phenols. Detection limits were significantly lower in negative ion than in positive ion mode. However, positive ion mode provided additional structural information for many of the compounds.</div>
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